Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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All bend tests require a tensile test machine or similar, with suitable grips and astn strength to bend the strongest alloy. Carbon and Sulfur Analysis. ASTM does not give any warranty express or implied or make any representation that the contents q262 this abstract are accurate, complete or up to date. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.
This method is a hour boiling test for “as received” specimens of stainless steel. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. SEP also gives guidance on which of its methods apply to which alloys: The latter is a German test, but it is often called up in European projects.
A recent publication on intergranular corrosion.
Intergranular Corrosion Tests for CRAs
For alloys not listed in this standard, it will be necessary to carry out some tests on material in various conditions to determine the threshold. Table 1 below shows the various methods for four common standards: Where a standard is included in a purchase specification, this must be followed, although it is advised that unsuitable tests, w262 as the Huey test for duplex and super austenitic stainless steels, are queried. It can be seen that some alloys fall into two categories, and no guidelines are given for selecting the most appropriate.
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ISO is the most rigorous in terms of defining test methods, and says which alloys should use which test methods as follows: Alternatively, a welded test-piece in the as-welded condition may be tested. Work Item s – proposed revisions of asmt standard.
Suggested test methods for different corrosion resistant alloys. Test Samples Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the asttm be a minimum of mm long. This abstract is a brief summary of the referenced standard. Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. There are other requirements in these standards over details that are not discussed in this document, and these should be followed, such as conducting bend tests.
Please refer to the specification for more details. It depends astmm which Practice is selected, but typically ranges from to days for different tests. For example, many low-carbon and stabilized stainless steels e. This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility. A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials.
The test solutions and exposures for some common intergranular corrosion tests. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively.
Both of these tests should be followed by water quenching.
It is informational only and not an official part of the standard; the w262 text of the standard itself must be referred to for its use and application.
ISO is the most rigorous in terms of defining test methods, and says which alloys should use which test methods as follows:. Link to Active This link will always route to the current Active version of the standard. When a test has been selected, follow the detailed directions in that standard for making up the test solution, the preparation of test samples and the finish to be used.
For many alloys, the onset is at 0.
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Intergranular Corrosion Testing: An Overview of ASTM A262
ISO is specifically for duplex and all austenitic stainless steels, and recommends ageing at two different temperatures: Some specific hazards statements are given in ASTM A was designed for austenitic stainless steels, specifically the series alloys. ASTM G28 method B is a more aggressive test than method A and is intended for more corrosion resistant alloys, as listed in the document. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. How do you select the right ASTM corrosion testing method for your material? The test uses a visual inspection of the atm of the bent specimen to determine pass or fail. Aatm exception to this is ASTM G28 method A, where rates for the onset of intergranular corrosion are described in reference 1.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
More suitable alternatives are offered in Table 5, below. Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack.
For an alloy that is not listed, look for an x262 with a similar composition to a listed alloy to determine the most suitable test. The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.
A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use.